A more refined method of obtaining cocaine involves treating the leaves with sodium carbonate solution, followed by treatment with dilute acid and descent with ether. The solvent is evaporated after which the substance is redissolved and subsequently crystallized (Considine, 1983, 89).
The rush in drug use in the United States in the 1970s and 1980s created a subculture in part dedicated to producing alternative or synthetic versions of drugs require under Schedule I and II, as wild or controlled (see Appendix I). There is one schedule (See Appendix II) for sale on the Internet that contains much of the pertinent information regarding the subtraction of cocaine from precursors. A close inspection of this document dates it from at least 1984, with a refreshment of the exact same document in 1994. However, this was not a revolutionary change world described. It has been well known for some time that synthetic cocaine could be manufactured from ecgonine [C9H15NO3] (Considine, 1983, 89). What is different, sociologically speaking, is that the knowledge of how to produce this dangerous and addictive drug, has become public knowledge, visavis the Internet.
The tropinones can be used in the higher up formula (or in a formula that you have build elsewhere) to be converted to cocaine. Remember to recrystallize the 2carbomethoxytropinone before converting to methyl group groupecgonine (Synthetic cocaine, 1997).
2Carbomethoxytropinone. A mixture of 1.35g of sodium methoxide (this is sodium in a minimum amount of methanol), 3.5g of tropinone, 4 ml of dimethylcarbonate and 10 ml of toluene is refluxed for 30 min. Coo] to 0? and add 15 ml of piddle that contains 2.5g of ammonium chloride. Extract the solution after vibe with four 50 ml portions of chloroform, dry, evaporate the chloroform in vacuo. Dissolve the crude residue in 100 ml of ether, wash twice with a mixture of 6 ml of saturated potassium carbonate and three ml of 3 N KOH.
Dry and evaporate in vacuo to recover the unreacted tropinone. direct up the oil in a solution of aqueous ammonium chloride and extract with chloroform, dry, and evaporate in vacuo to get an oil. The oil is dissolved in hot acetone, cool, and scratch inside of flaskful with glass rod to precipitate 2 carbomethoxytropinone. Recrystallize 16 g of this product in 30 ml of hot methyl acetate and add 4 ml of cold water and 4 ml of acetone. Put in freezer for 2l/2 to 3 hours. Filter and wash the precipitate with cold methyl acetate to get pure product.
pby rate process of double and triple replacement. The instructions break eat up into four sets of linked processes, each with subcategories involving synthesizing the ingredients needed to produce synthetic cocaine. In short, the author indicates that tropinone be converted first into 2carbomethoxytropinine (meytheltropon3one2carbonate). Next 2carbomethoxytropinine needfully to converted to ecgonine and ecgonine into cocaine (see below). The instructions come with the warning that the process is not easy. Indeed, anyone not familiar with the equipment and procedures would do well to leave things alone.
Step two is about converting succindiald
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